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The catalytic process involving use of
Palladium on Charcoal ( a heterogeneous type of catalyst ) the
separation of catalyst from the products of the reaction is quite
easy. Most of the catalyst particles after the stoppage of
agitator, settles at the bottom of the reactor under the influence
of gravity.
A small fraction constituting less
than two / three percent may however remain in suspended
form. The products of reaction being in liquid form can be
subjected to filtration using notch filter with filter cloth
having pore size of less than 15 microns. A filter paper
sheet may also be spread over the filter cloth to assist clear
filtration.
Initially some catalyst particles
may pass through filter cloth. Such portion of the filtered
liquid should be subjected to refiltration. In case of small
volumes, use of centrifuge may be mixed with the bulk quantity of
catalyst lying in the reactor. However it should be ensured
that catalyst particles collected on the filter paper or filter
cloth do not get dried up as dried particles may catch fire. |